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中文名稱(chēng):Marine Sediment Inorganic Sediment
英文名稱(chēng):Marine Sediment Inorganic Sediment訂貨以英文名稱(chēng)為準(zhǔn)。
產(chǎn)品編號(hào):IAEA-459CAS:/
品牌:標(biāo)準(zhǔn)物質(zhì)產(chǎn)地:進(jìn)口
標(biāo)準(zhǔn)值:見(jiàn)證書(shū)分子式:/
規(guī)格 市場(chǎng)價(jià)(元) 折后價(jià)(元) 供貨周期 數(shù)量 加入購(gòu)物車(chē) 50g 0.00 0.00 3-4周 加入購(gòu)物車(chē)
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產(chǎn)品詳細(xì)介紹
IAEA-459Marine Sediment Inorganic Sediment
Origin and preparation of the material
A marine sediment sample was collected in Han River estuary, South Korea. This sediment was freeze-dried, ground and sieved at 125 μm.
The sieved sediment obtained, around 26 kg, with a particle size of less than 125 μm was homogenized by mixing it in a stainless steel rotating homogenizer for three weeks. Then, aliquots of about 50 g were packaged into cleaned amber glass bottles with aluminium screw caps, labelled IAEA-459 and sealed with Teflon tape.
This certified reference material is intended to be used as a quality control material for the assessment of a laboratory’s analytical work, for the development and validation of analytical procedures, and for quality assurance within a laboratory in the determination of chlorinated pesticides, PCBs, polybrominated diphenyl ethers and polycyclic aromatic hydrocarbons in sediment samples with very low concentration levels.
Certified mass fractions values
(based on dry mass)
Polycyclic Aromatic hydrocarbonsAnalyte Unit Certified value1 Expanded uncertainty2 2-Methylnaphthalene μg kg-1 15.5 5.0 1-Methylnaphthalene μg kg-1 9.2 3.6 Acenaphthylene μg kg-1 3.2 1.3 Fluorene μg kg-1 4.7 1.9 Acenaphthene μg kg-1 1.78 0.73 Dibenzothiophene μg kg-1 9.4 1.8 Phenanthrene μg kg-1 33.9 6.0 Anthracene μg kg-1 6.0 1.0 Fluoranthene μg kg-1 37.3 3.0 Pyrene μg kg-1 46.3 8.3 Benz(a)anthracene μg kg-1 19.3 4.3 Chrysene+triphenylene μg kg-1 27.5 8.5 Benzo(b)fluoranthene μg kg-1 44.1 9.3 Benzo(b+j) fluoranthene μg kg-1 59 15 Benzo(k)fluoranthene μg kg-1 19.0 5.3 Benzo(e)pyrene μg kg-1 36 12 Benzo(a)pyrene μg kg-1 22.7 4.3 Indeno[1,2,3-c,d]pyrene μg kg-1 36 11 Benzo(g,h,i)perylene μg kg-1 36 11
PCB congenersAnalyte Unit Certified value1 Expanded uncertainty2 PCB 28 μg kg-1 2.27 0.56 PCB 31 μg kg-1 2.41 0.60 PCB 44 μg kg-1 1.72 0.64 PCB 49 μg kg-1 2.64 0.40 PCB 52 μg kg-1 2.38 0.67 PCB 66 μg kg-1 3.10 0.81 PCB 87 μg kg-1 1.24 0.17 PCB 101 μg kg-1 3.78 0.43 PCB 105 μg kg-1 1.29 0.31 PCB 110 μg kg-1 3.70 0.68 PCB 118 μg kg-1 2.98 0.39 PCB 128 μg kg-1 0.62 0.11 PCB 138 μg kg-1 3.25 0.89 PCB 149 μg kg-1 2.88 0.51 PCB 151 μg kg-1 0.66 0.18 PCB 153 μg kg-1 3.75 0.66 PCB 156 μg kg-1 0.336 0.063 PCB 170 μg kg-1 1.02 0.22 PCB 180 μg kg-1 2.22 0.34 PCB 183 μg kg-1 0.72 0.27 PCB 187 μg kg-1 1.39 0.20 PCB 209 μg kg-1 0.199 0.067 Chlorinated pesticides
Analyte Unit Certified value1 Expanded uncertainty2 pp' DDE μg kg-1 3.60 0.48 pp' DDD μg kg-1 3.00 0.93 pp' DDT μg kg-1 1.32 0.52 op DDE μg kg-1 0.47 0.11 op DDD μg kg-1 0.75 0.27 op DDT μg kg-1 0.35 0.13 PBDE congeners
Analyte Unit Certified value1 Expanded uncertainty2 BDE 47 μg kg-1 0.177 0.060 BDE 99 μg kg-1 0.240 0.067 BDE 153 μg kg-1 0.097 0.022 BDE 183 μg kg-1 0.282 0.065 BDE 209 μg kg-1 10.8 2.9 1) The value is the robust mean of accepted sets of data, each set being obtained by different laboratory. The certified values are reported on dry mass basis and are traceable to the SI.
2) Expanded uncertainty with a coverage factor k=2 2 Expanded uncertainty with a coverage factor k=2 estimated in accordance with the JCGM 100:2008 Evaluation of measurement data – Guide to the expression of uncertainty in measurement [1], corresponding to the level of confidence of about 95%.